Characterization of Transition Metal Dichalcogenide Nanostructures Synthesized by Liquid-Phase Controlled Fusion Technique
DOI:
https://doi.org/10.2025/b8n31475Abstract
In this letter, the synthesis of MoSSe nanosheets by liquid-phase controlled fusion technique is presented. The liquid-phase reaction of transition metal (Mo) with two chalcogenides (S and Se) was initiated in an inert environment and organic solvent. The synthesized material exhibited a polycrystalline structure with no traces for free elements or other phases than MoSSe and preferred parallel orientations, which confirmed the formation of nanosheets. Also, the elemental analysis showed that the synthesized material is sufficiently pure. The spectroscopic analysis confirmed the formation of all bonds required to form the MoSSe lattice. This attempt can be considered to synthesize nanosheets from hybrid systems based on transition metal and dichalcogenides.
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